Acutifoliside, a novel benzoic acid glycoside from Salix acutifolia

A - Papers appearing in refereed journals

Wu, Y., Dobermann, D., Beale, M. H. and Ward, J. L. 2016. Acutifoliside, a novel benzoic acid glycoside from Salix acutifolia. Natural Product Research. 30 (15), pp. 1731-1739.

AuthorsWu, Y., Dobermann, D., Beale, M. H. and Ward, J. L.
Abstract

Ultra high-performance liquid chromatography–mass spectrometry (UHPLC–MS) profiling of a polar solvent extract of juvenile stem tissue of Salix acutifolia Willd. identified a range of phenolic metabolites. Salicortin, 1, a well-known salicinoid, was the major compound present and the study identified young stem tissue of this species as a potential source of this compound for future studies. Three further known metabolites (salicin 2, catechin 3 and tremuloidin 4) were also present. The UHPLC–MS analysis also revealed the presence of a further, less polar, unknown compound, which was isolated via HPLC peak collection. The structure was elucidated by high-resolution mass spectroscopic analysis, 1- and 2-D NMR analysis and chemical derivatisation and was shown to be a novel benzoic acid glycoside 5, which we have named as acutifoliside.

Year of Publication2016
JournalNatural Product Research
Journal citation30 (15), pp. 1731-1739
Digital Object Identifier (DOI)doi:10.1080/14786419.2015.1137571
Open accessPublished as non-open access
FunderBiotechnology and Biological Sciences Research Council
Engineering and Physical Sciences Research Council
Funder project or codeSupport
Cropping Carbon (CC) [ISPG]
Sustainability
Maximising carbon harvest from perennial crops
Ionic Liquid Biorefining of Lignocellulose to Sustainable Polymers
PBSC Metabolomics and Metabolite Facilities
Ionic Liquid Biorefining of Lignocellulose to Sustainable Polymers
*BBSRC Notts DTP:Darja Doberman
Output statusPublished
Publication dates
Online28 Jan 2016
Publication process dates
Accepted02 Dec 2015
PublisherTaylor & Francis
Taylor & Francis
ISSN1478-6419

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