A comparison of X‐ray fluorescence spectrometry and chemical methods for determining sulphur in plant material

A - Papers appearing in refereed journals

Bolton, J., Brown, G., Pruden, G. and Williams, C. 1973. A comparison of X‐ray fluorescence spectrometry and chemical methods for determining sulphur in plant material. Journal of the Science of Food and Agriculture. 24, pp. 577-563. https://doi.org/10.1002/jsfa.2740240509

AuthorsBolton, J., Brown, G., Pruden, G. and Williams, C.
Abstract

A rapid method for determining total S in plants by X‐ray fluorescence spectro‐metric analysis of ground pelletised plant material is compared with chemical methods using titrimetric, flame photometric and turbidimetric methods of sulphate determination. Errors in the chemical methods were caused by incomplete oxidation of organic sulphur and by non‐reproducibility of the turbidimetric determination of sulphate. A method incorporating the oxidation of the sample with HNO3 and Mg(NO3)2 and titration of the reduced sulphate by mercuric acetate gave recoveries accurate to a mean of 1% when determining the sulphur content of sulphur compounds.

RESP-6757

Year of Publication1973
JournalJournal of the Science of Food and Agriculture
Journal citation24, pp. 577-563
Digital Object Identifier (DOI)https://doi.org/10.1002/jsfa.2740240509
Open accessPublished as non-open access
Output statusPublished
PublisherWiley
ISSN0022-5142

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